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Displaying 1551 - 1575 of 4041

International Comparison of a Hydrocarbon Gas Standard at the Picomol per Mol Level

February 6, 2014
Author(s)
George C. Rhoderick, David L. Duewer, Eric Apel, Annarita Baldan, Bradley Hall, Alice Harling, Detlev Helmig, Gwi S. Heo, Jacques Hueber, Mi E. Kim, Yong D. Kim, Benjamin Miller, Stephen Montzka, Daniel Reimer
Studies of climate change increasingly recognize the diverse influences of hydrocarbons in the atmosphere, including roles in particulates and ozone formation. Measurements of key non methane hydrocarbons (NMHCs) suggest atmospheric mole fractions ranging

CPTAC Studies 1 and 5: dissecting variability in multi-site LC-MS/MS proteomics through quality metrics and robust hierarchical multivariate statistics

February 4, 2014
Author(s)
Stephen E. Stein, David M. Bunk, Xia Wang, Matthew Chambers, Lorenzo J. Vega-Montoto, David L. Tabb
Shotgun proteomics experiments integrate a complex sequence of processes, any of which can introduce variability. Quality metrics computed from LC-MS/MS data have relied upon identifying MS/MS scans, but a new mode for the QuaMeter software produces

Estimation of the Limit of Detection Using Information Theory Measures

January 31, 2014
Author(s)
Alexander (. Vergara Tinoco, Fonollosa Jordi, Huerta Ramon, Santiago Marco
Definitions of the Limit of Detection (LoD) based on the probability of false positive and/or false negative errors have been proposed over the past years. Although such definitions are straightforward and valid for any kind of analytical system, the

Quantification of total serum transferrin and transferrin sialoforms in human serum; an alternative method for the determination of carbohydrate-deficient transferrin in clinical samples

January 20, 2014
Author(s)
Yoana Y. Nuevo Ordonez, William C. Davis, Raymond F. Anton
Carbohydrate deficient transferrin (CDT) measurements in human serum constitute the most specific marker for chronic heavy alcohol use and congenital disorders of glycosylation in proteins. Therefore, the development of precise and accurate analytical

Measuring order in regioregular poly(3-hexylthiophene) with solid-state 13C CPMAS NMR

January 10, 2014
Author(s)
Ryan C. Nieuwendaal, Chad R. Snyder, Dean M. DeLongchamp
We report on details of molecular packing in high molar mass poly(3-hexylthiophene) (P3HT) by solid-state 13C {1H} cross-polarization magic angle spinning (CPMAS) NMR measurements. The degree of polymer order was estimated for two films of varied drying

Influence of tissue, age, and environmental quality on global levels of genomic methylation in the American alligator (Alligator mississippiensis)

January 7, 2014
Author(s)
Benjamin B. Parrott, John Bowden, Satomi Kohno, Jessica A. Cloy-McCoy, Jacqueline T. Bangma, Thomas R. Rainwater, Phillip M. Wilkinson, John Kucklick, Louis J. Guillette
Epigenetic modifications are key mediators of the interactions between the environment and an organism's genome. DNA methylation represents the best-studied epigenetic modification to date and is known to play key roles in regulating transcriptional

Probing the intracellular glutathione redox potential using in-cell NMR spectroscopy

January 2, 2014
Author(s)
Steve Y. Rhieu, Aaron A. Urbas, Daniel W. Bearden, John P. Marino, Vytautas Reipa, Katrice A. Lippa
Non-invasive and real-time analysis of cellular redox processes has been greatly hampered by lack of suitable measurement techniques. Here we describe an in-cell nuclear magnetic resonance (NMR)-based method for measuring the intracellular glutathione

Nonlinear Vibrational Spectrometry

December 31, 2013
Author(s)
Lee J. Richter
Second order nonlinear spectroscopies such as sum frequency generation (SFG) are intrinsically interface sensitive and enable sub monolayer sensitivity to be achieved at buried, optically accessible interfaces. Vibrationally-resonant SFG allows bond

Correlation of rocket propulsion fuel properties with chemical composition using comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry followed by partial least squares regression analysis

December 30, 2013
Author(s)
Thomas J. Bruno, Benjamin Kehimkar, Jamin C. Hoggard, Luke C. Marney, M. C. Billingsley, C. G. Fraga, R. E. Synovec
There is an increased need to more fully assess and control the composition of kerosene-based rocket propulsion fuels such as RP-1. In particular, it is critical to make better quantitative connections among the following three attributes: fuel performance
Displaying 1551 - 1575 of 4041
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