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Displaying 901 - 925 of 4041

Mass Spectral Library Quality Assurance by Inter-Library Comparison

April 2, 2017
Author(s)
William E. Wallace, Weihua Ji, Dmitrii V. Tchekhovskoi, Karen W. Phinney, Stephen E. Stein
A method to discover and correct errors in mass spectral libraries is described. Comparing across a set of highly curated reference libraries compounds that have the same chemical structure quickly identifies entries that are outliers. In cases where three

Quantifying Stability of Trace Explosives under Different Environmental Conditions

April 1, 2017
Author(s)
Edward R. Sisco, Marcela N. Najarro, Daniel V. Samarov, Jeffrey A. Lawrence
This work investigates the stability of trace deposits of six explosives (ETN, PETN, RDX, HMX, TNT, and Tetryl) to determine environmental stabilities and lifetimes. Explosives were inkjet printed directly onto PTFE coated fiberglass substrates and exposed

Liquid Chromatography Column Theory and Technology

March 8, 2017
Author(s)
Lane C. Sander
Column selection is probably the single most important aspect of method development that will directly affect measurement accuracy and precision of liquid chromatographic (LC) measurements. An understanding of physical and chemical properties of LC columns

Liquid Chromatography: Introduction to Method Development

March 8, 2017
Author(s)
Lane C. Sander
The development of fit-for-purpose analytical methods is an essential component of chemical metrology. This presentation will provide guidance on approaches for establishing robust analytical methods, particularly with applications to liquid chromatography

Solid Phase Extraction

March 8, 2017
Author(s)
Lane C. Sander
Solid Phase Extraction [video, running time 29 minutes 2 seconds] \\europa\839.02\training\Solid Phase Extraction (29.02 minutes).mp4 Lane C. Sander Chemical Sciences Division Material Measurement Laboratory National Institute of Standards and Technology

Expanding lipidome coverage using LC-MS/MS data-dependent acquisition with automated exclusion list generation

March 6, 2017
Author(s)
John Bowden, Jeremy P. Koelmel, Nicholas M. Kroeger, Emily L. Gill, Candice Z. Ulmer, Rainey E. Patterson, Richard A. Yost, Timothy J. Garrett
Untargeted omics analyses aim to comprehensively characterize biomolecules within a biological system. Changes in the presence or quantity of these biomolecules can indicate important biological perturbations, such as those caused by disease. With current

Characterization of a PXIe based low-field digital NMR spectrometer

February 25, 2017
Author(s)
Joshua R. Biller, Karl F. Stupic, Anthony B. Kos, Timothy Weilert, George Rinard, Yoshi Nakashima, John M. Moreland
A low-field nuclear magnetic resonance (NMR) instrument is an important tool for investigating a wide variety of samples under different conditions. In this paper, we describe a system constructed primarily with commercially available hardware and control
Displaying 901 - 925 of 4041
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