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Metrology

Flow metrology & rheology

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Displaying 1 - 25 of 177

Estimating How Big: The Metric Estimation Game

July 30, 2025
Author(s)
Elizabeth Benham, Kristen Dill, Dinelka Jagoda, Maryanne Amanze, Yoon Thwel
The metric system (International System of Units, SI) is easy to use and learn. The Metric System Estimation Game is a fun, hands-on activity that helps participants become familiar with SI measurements by practicing estimation skills. During this activity

Rheology and Microstructural Behavior of Semidilute Suspensions of Semiflexible Rods across Five Decades of Shear Rate

February 18, 2025
Author(s)
Paul Salipante, Ryan Murphy, Steve Kuei, Jeffrey Fagan, Christopher Sims, Kathleen Weigandt, Steven Hudson
Rod-like particles are efficient rheology modifiers and are commonly found in a variety of biological and industrially relevant suspensions, from biofilaments to worm-like surfactant micelles. These suspensions display strong shear-thinning behavior, and

Calibrating laser Doppler anemometers utilizing an optical chopper

January 31, 2025
Author(s)
Christopher Crowley, Iosif Isaakovich Shinder, Michael R. Moldover, Joey Boyd, James Filla, Aaron Johnson
Laser Doppler anemometers (LDAs) use scattered light to determine velocity components of a flowing fluid. The operating principal of LDAs is simple conceptually; however, it is impractical to trace the LDA-determined velocities to the SI by characterizing

Two-fluid model for nonlinear flow of wormlike micelle solutions. II: Experiment

November 1, 2024
Author(s)
Paul Salipante, Michael Cromer, Steven D. Hudson
Applications often expose wormlike micelle solutions to a very wide range of shear and temperature conditions. The two-species model presented in Part I [Salipante et al., J. Rheol. 68 (2024)] describes the nonlinear rheology over a wide range of shear

Entanglement kinetics in polymer melts are chemically specific

July 3, 2024
Author(s)
Benjamin Dolata
We investigate the universality of entanglement kinetics in polymer melts. We compare predictions of a recently developed constitutive equation for disentanglement to molecular dynamics simulations of both united-atom polyethylene and Kremer-Grest models

Evaluating Models That Predict Epoxy Conversion Using Rheological Properties

April 15, 2024
Author(s)
Stian Romberg, Paul Roberts, Chad R. Snyder, Anthony Kotula
Simultaneous rheology and conversion measurements of neat and composite epoxy resins reveal that conventional models neither accurately nor fully describe the relationship between rheology and conversion. We find that models predicting thermoset conversion

Non-nulling Protocols for Fast, Accurate, 3-D Velocity Measurements in Stacks

July 28, 2023
Author(s)
Iosif Isaakovich Shinder, Aaron Johnson, James Filla, Vladimir B. Khromchenko, Michael R. Moldover, Joey Boyd, John D. Wright, John R. Stoup
We present protocols for making fast, accurate, 3-D velocity measurements in the stacks of coal-fired power plants. The measurements are traceable to internationally-recognized standards; therefore, they provide a rigorous basis for measuring and/or

Dynamic Measurement of Gas Flow using Acoustic Resonance Tracking

March 21, 2023
Author(s)
Jodie Gail Pope, Keith A. Gillis, James W. Schmidt
We measured gas flows exiting large, un-thermostated, gas-filled, pressure vessels by tracking the time-dependent pressure P(t) and resonance frequency fN(t) of an acoustic mode N of the gas remaining in each vessel. This is a proof-of-principle

Microfluidic techniques for mechanical measurements of biological samples

January 20, 2023
Author(s)
Paul Salipante
The use of microfluidics to make mechanical property measurements is increasingly common. Fabrication of microfluidic devices has enabled various types of flow control and sensor integration at micrometer length scales to interrogate biological materials

Gas Flow Standards and Their Uncertainty

December 12, 2022
Author(s)
John D. Wright, Aaron Johnson, Michael R. Moldover, Shin-ichi Nakao
We review diverse types of gas flow standards that are used to calibrate other gas flow meters. For each type of standard, we describe the principles of its operation and at least one hardware example. We identify the practical limits of the example's

SerialTrack: ScalE and Rotation Invariant Augmented Lagrangian Particle Tracking

September 19, 2022
Author(s)
Jin Yang, Yue Yin, Alexander Landauer, Selda Buyukozturk, Jing Zhang, Luke Summey, Alexander McGhee, Matthew Fu, John Dabiri, Christian Franck
We present a new particle tracking algorithm to accurately resolve large deformation and rotational motion fields, which takes advantage of both local and global particle tracking algorithms. We call this method the ScalE and Rotation Invariant Augmented

Overcoming Technological Barriers in Microfluidics: Leakage Testing

September 1, 2022
Author(s)
Vania Silverio, Suvajyoti Guha, Armelle Keiser, Rucha Natu, Darwin Reyes-Hernandez, Henne van Heeren, Nicolas Verplanck, Luke Herbertson
The miniaturization of laboratory procedures for Lab-on-Chip (LoC) devices and translation to various platforms such as single cell analysis or Organ-on-Chip (OoC) systems are revolutionizing the life sciences and biomedical fields. As a result

A small-volume microcapillary rheometer

March 30, 2022
Author(s)
Paul Salipante, Steve Kuei, Steven Hudson
We demonstrate a capillary device used to measure the shear rate dependent viscosity of microliter scale volumes. Liquid samples are driven pneumatically to fill a microcapillary and partially fill a larger glass capillary. The glass capillary is mounted

Disinfection of Respirators with Ultraviolet Radiation

March 25, 2022
Author(s)
Dianne L. Poster, Matthew Hardwick, C Cameron Miller, Michael A. Riley, W. W. Shanaka I. Rodrigo, Andras E. Vladar, John D. Wright, Christopher D. Zangmeister, Clarence Zarobila, Jeremy Starkweather, John Wynne, Jason Yilzarde
Data for interpreting virus inactivation on N95 face filtering respirators (FFRs) by ultraviolet (UV) radiation are important in developing UV strategies for N95 FFR disinfection and reuse for any situation, whether it be everyday practices, contingency

Optofluidic Flow Meter for sub-nanoliter per minute flow measurements

January 31, 2022
Author(s)
Jalal Sadeghi, Paul Patrone, Anthony J. Kearsley, Gregory A. Cooksey
Performance improvements in microfluidic systems depend on accurate measurement and control of fluids on the micro- and nanoscale, and new applications are continuously moving the needle to lower volumetric flow rates. This work focuses on improving an

Thermal Boundary Layers in Critical Flow Venturis

July 30, 2021
Author(s)
John D. Wright, Aaron Johnson, Michael R. Moldover, Woong Kang, Liang Zhang, Bodo Mickan
We improve the usefulness of small (diameter 10 mm) critical flow venturis (CFVs) as transfer standards for gas flow by measuring and explaining how their discharge coefficients depend on the temperature T of their environment. At Reynolds numbers Re 2.5

Blow-Down Calibration of a Large Ultrasonic Flow Meter

April 21, 2021
Author(s)
Aaron Johnson, Eric Harman, Joey Boyd
Oil and gas production industries use large (diameter > 0.8 m) ultrasonic flow meters (USMs) to measure exhaust gas from flare stacks, emissions from smokestacks, flow of natural gas, etc. Since most flow laboratories do not have compressors with

Accelerating Innovation and Commercialization Through Standardization of Microfluidic-Based Medical Devices

January 5, 2021
Author(s)
Darwin R. Reyes-Hernandez, Henne van Heeren, Suvajyoti Guha, Luke Herbertson, Alexios P. Tzannis, Jens Ducr?e, Hugo Bissig, Holger Becker
The microfluidics industry has grown steadily over the last 5 years worldwide, with the market for microfluidic medical devices experiencing a compound growth rate of 18%. The number of submissions to regulatory agencies such as the U.S. Food & Drug

Calibration Procedures for Orthogonal Superposition Rheology

November 18, 2020
Author(s)
Ran Tao, Aaron M. Forster
Orthogonal superposition (OSP) rheology is an advanced rheological technique that involves superimposing a small-amplitude oscillatory shear deformation orthogonal to a primary shear flow. This technique allows the measurement of structural dynamics of
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