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William Dinis Camara, Steven J. Choquette, Katya Delak, Robert Hanisch, Benjamin Long, Melissa M. Phillips, Jared Ragland, Kate Rimmer
Early in 2022 NIST embarked on a pilot project to produce digital calibration reports and digital certificates of analysis for reference materials. The goal of the project is to produce a few examples of digital reports and certificates for the purpose of
The review covers wide-ranging electron ionization (EI) dissociation reactions for various acyclic compounds and their derivatives such as alcohols, aldehydes, ketones, carboxylic acids, amines, halides, thiols, thiones, esters, thioesters, amides and more
Jamie Weaver, Anna Job, Kedar Manandhar, Ichiro Takeuchi, Robert Gregory Downing
A protective covering is often required for neutron depth profiling (NDP) measurements of sensitive materials (e.g., Li-ion batteries). Addition of this layer can increase NDP profile energy broadening and depth assignment uncertainty. This study evaluates
We have investigated the use of negative molecular oxygen primary ion beams (i.e., O2- and O3-) to determine the benefits of using such beams for uranium particle SIMS analyses. Typically, O- is the most practical negative primary ion species for both age
Vania Silverio, Suvajyoti Guha, Armelle Keiser, Rucha Natu, Darwin Reyes-Hernandez, Henne van Heeren, Nicolas Verplanck, Luke Herbertson
The miniaturization of laboratory procedures for Lab-on-Chip (LoC) devices and translation to various platforms such as single cell analysis or Organ-on-Chip (OoC) systems are revolutionizing the life sciences and biomedical fields. As a result
Akim Babenko, Nathan Flowers-Jacobs, GREGOR LASSER, Justus Brevik, Anna Fox, Paul Dresselhaus, Zoya Popovic, Samuel P. Benz
We present the design, fabrication and characterization of a broadband RF Josephson Arbitrary Waveform Synthesizer (RF-JAWS) with a series array of 4500 Josephson junctions (JJs) and integrated low-pass/high-pass five-pole superconducting diplexers. The
This document, SP250-99 (2022), NIST Measurement Services: Diffuse Visual Transmission Density, describes the instrument used to measure diffuse visual transmission density of both x-ray and photographic film step tablets. These step tablets replace former
Archita Hati, Marco Pomponio, Connor Humiston, John Lettang, Craig Nelson
We report the performance of a 30 GHz to 10 GHz regenerative frequency divider. The proposed divider design incorporates the conventional Miller regenerative frequency divider (divide-by-2) with an additional regenerative path. We achieve output referred
Nicholas G. Paulter Jr., Ioan Tudosa, Francesco Picariello, Pasquale Daponte, Luca De Vito, Sergio Rapuano
A prototype implementation of a phase measurement method (PMM) for a sine-wave signal delivered at the output port of a generator and its experimental assessment is presented. This PMM is capable of measuring the output phase of a sine-wave signal respect
Eliad Peretz, Peter Plavchan, Piotr Pachowicz, Jamie Tayar, Gerard van Belle, Greg Aldering, Angelle Tanner, Justin Albert, Daniel Huber, Leonard Hanssen, Brian Alberding, Joseph P. Rice, Steven West, John Mather, Allison Youngblood, Tabetha Boyajian, Brian Stalder, Jonathan Gagne, Susana Deustua, Kayla Carmical, Andrew Lewis
This paper describes the scientific and developmental aspects behind the QUAsi-Stationary Absolute Radiance (QUASAR) mission study. The scientific motivation on which the mission is built is established, including the absolute flux calibration of standard
Alexander Tzalenchuk, Nicolas Spethmann, Tim Prior, Jay H. Hendricks, Yijie Pan, Vladimir Bubanja, Guilherme Temporao, Dai-Hyuk Yu, Damir Ilic, Barbara L. Goldstein
Now that all base units are defined in terms of fundamental constants and can thus — at least in principle — be realized anytime and anywhere, rather than through a measurement chain leading back to unique physical artefacts, who holds the traceability
We present a simple method for the adjustment of an in-phase (I) and quadrature-phase (Q) Armstrong type modulator for use as a calibrator in precision noise metrology. The availability of relatively pure levels of both amplitude modulation (AM) and phase
Papa Amoah, Pentao Lin, Zeinab Mohammed Hassan, Rhonda Franklin, Engelbert Redel, Helmut Baumgart, Yaw S. Obeng
Changes in the chemo-electrical intrinsic properties of metal-oxide materials (MO) are commonly used as the basis of gas sensors. The most common gas sensors are based on chemically induced changes in electrical resistivity which necessarily involve making
For hydrogen-deuterium exchange mass spectrometry (HDX-MS) to have an increased role in quality control of biopharmaceuticals, H for D back-exchange occurring during protein analyses should be minimized to promote greater reproducibility. Standard HDX-MS
Marcia L. Huber, Eric W. Lemmon, Ian Bell, Mark O. McLinden
The NIST REFPROP database is a powerful tool for calculating thermophysical properties of industrially important fluids, and this manuscript describes the models implemented in, and features of, this database. REFPROP implements the most accurate models
Stephan Schlamminger, Leon Chao, Vincent Lee, David B. Newell, Clive Speake
The torsion pendulum at the heart of the BIPM apparatus to measure the gravitational constant, $G$, is used to measure the gravitational torque between source and test-mass assemblies with two methods. In the Cavendish method, the pendulum moves freely. In
Solomon I. Woods, Jorge Neira, James E. Proctor, Joseph P. Rice, Nathan Tomlin, Malcolm White, Michelle Stephens, John H. Lehman
We have developed generalized methods for electrical substitution optical measurements, as well as cryogenic detectors which can be used to implement them. The new methods enable measurement of arbitrary periodic waveforms by an electrical substitution
A new fundamental equation of state is presented for 2,3,3,3-tetra uoroprop-1-ene (R1234yf). The equation is valid from the triple point temperature (121.6 K) to 410 K at pressures up to 100 MPa, where typical expanded uncertainties (k = 2) in calculated
Zane Comden, Stephan Schlamminger, Charles Waduwarage Perera, Frank Seifert, David B. Newell, Jay H. Hendricks, Barbara L. Goldstein, Leon Chao
After the 2019 redefinition of the International System of Units (SI), torque no longer needs to be traceable to a calibrated weight suspended from a known lever arm. Specifically, a modification of the Kibble principle used for realizing the kilogram
A simple model is presented for multi-point normalization of dual-inlet isotope ratio mass spectrometry (DI-IRMS) data. The model incorporates the scale contraction coefficient and the normalized working reference gas isotope delta value as its two
There is a pressing need for reliable, reproducible and accurate measurements of graphene's properties. To facilitate industrial growth, several documentary measurement standards are under development within the Nanotechnologies committees of both ISO 229
Tom Parker, Victor Zhang, Jian Yao, Gerard Petit, Roger Brown, James Hanssen
A three-cornered hat analysis has been performed on three independent time transfer systems between the United States Naval Observatory (USNO) and the National Institute of Standards and Technology (NIST). These include (1) a direct Two-Way Satellite Time
Elijah Petersen, Richard Uhl, Blaza Toman, John Elliott, John Gordon
Background: The Electrophilic Allergen Screening Assay (EASA) has emerged as a promising method for risk and hazard assessment for skin sensitization classification. This assay functions by assessing the depletion of one of two probe molecules (4
Single-photon detection via absorption in current-biased nanoscale superconducting structures has become a preferred technology in quantum optics and related fields. Single-mode fiber packaged devices have seen new records set in detection efficiency