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There remains a need for rheological characterization of metal powder used for powder-spreading-based additive manufacturing (AM). Novel powder rheometers introduced to the commercial market for this purpose must be rigorously evaluated for repeatability
Takehiko Oe, Shamith Payagala, Alireza Panna, S. Takada, N. Kaneko, Dean G. Jarrett
A precise high resistance comparison was performed between the traveling dual source bridge developed by the National Metrology Institute of Japan (NMIJ) and the Adapted Wheatstone Bridge of the National Institute of Standards and Technology (NIST) from 10
The metrological definition of traceability for a GPSDO or GPSDC requires an unbroken series of measurements to a national standard, with known uncertainties at each step. The calibrations must be end-to-end, including the antenna and cabling. While
Stephan Schlamminger, Lorenz Keck, Frank Seifert, Leon Chao, Darine El Haddad, Shisong Li
Analytically the force and torques on a coil in a field of magnetic flux density can be calculated one of two ways. The line integral can be conducted along the coil's wire, summing up the differential force contribution. For each differential line segment
David Sefcik, Katrice Lippa, N. Alan Heckert, Stephen Benjamin, Ivan Hankins, Don Onwiler
The National Conference on Weights and Measures (NCWM) in partnership and cooperation with the NIST Office of Weights and Measures (OWM) and the Weights and Measures Divisions of select U.S. States initiated the 2022 National Survey on 20 lb LPG (Propane)
Kaleb Duelge, George Mulholland, Vincent A. Hackley, Michael Zachariah
A critical and extensive comparison was made between differential mobility analysis (DMA) measurements of the mean diameter of monodisperse gold nanoparticles (AuNP), based on step-voltage mode and the more commonly used scan-voltage mode (commercially
Lorenz Keck, Frank Seifert, David B. Newell, Rene Theska, Darine El Haddad
A quantum electro-mechanical metrology suite (QEMMS) is being built at the National Institute of Standards and Technology (NIST). As the first instrument in his class, the QEMMS combines all three, a programmable Josephson voltage system, a quantum Hall
Linsey Rodenbach, Alireza Panna, Shamith Payagala, Ilan Rosen, Molly Andersen, Joseph Hagmann, Peng Zhang, Lixuan Tai, Kang Wang, Dean G. Jarrett, Randolph Elmquist, Jason Underwood, David B. Newell, David Goldhaber-Gordon, Albert Rigosi
Catherine Cooksey, James A. Fedchak, Robert Hanisch, Gregory (Greg) C. Cala, Damian Lauria, Raymond Plante, Benjamin Long, John S. Quintavalle, Manmohan Moodra
Early in 2022 NIST embarked on a pilot project to produce digital calibration reports and certificates of analysis for reference materials. The goal of the project was to produce a few examples of each for the purpose of assessing the scope and challenges
William Dinis Camara, Steven J. Choquette, Katya Delak, Robert Hanisch, Benjamin Long, Melissa M. Phillips, Jared Ragland, Kate Rimmer
Early in 2022 NIST embarked on a pilot project to produce digital calibration reports and digital certificates of analysis for reference materials. The goal of the project is to produce a few examples of digital reports and certificates for the purpose of
The review covers wide-ranging electron ionization (EI) dissociation reactions for various acyclic compounds and their derivatives such as alcohols, aldehydes, ketones, carboxylic acids, amines, halides, thiols, thiones, esters, thioesters, amides and more
Jamie Weaver, Anna Job, Kedar Manandhar, Ichiro Takeuchi, Robert Gregory Downing
A protective covering is often required for neutron depth profiling (NDP) measurements of sensitive materials (e.g., Li-ion batteries). Addition of this layer can increase NDP profile energy broadening and depth assignment uncertainty. This study evaluates
We have investigated the use of negative molecular oxygen primary ion beams (i.e., O2- and O3-) to determine the benefits of using such beams for uranium particle SIMS analyses. Typically, O- is the most practical negative primary ion species for both age
Vania Silverio, Suvajyoti Guha, Armelle Keiser, Rucha Natu, Darwin Reyes-Hernandez, Henne van Heeren, Nicolas Verplanck, Luke Herbertson
The miniaturization of laboratory procedures for Lab-on-Chip (LoC) devices and translation to various platforms such as single cell analysis or Organ-on-Chip (OoC) systems are revolutionizing the life sciences and biomedical fields. As a result
Akim Babenko, Nathan Flowers-Jacobs, GREGOR LASSER, Justus Brevik, Anna Fox, Paul Dresselhaus, Zoya Popovic, Samuel P. Benz
We present the design, fabrication and characterization of a broadband RF Josephson Arbitrary Waveform Synthesizer (RF-JAWS) with a series array of 4500 Josephson junctions (JJs) and integrated low-pass/high-pass five-pole superconducting diplexers. The
This document, SP250-99 (2022), NIST Measurement Services: Diffuse Visual Transmission Density, describes the instrument used to measure diffuse visual transmission density of both x-ray and photographic film step tablets. These step tablets replace former
Archita Hati, Marco Pomponio, Connor Humiston, John Lettang, Craig Nelson
We report the performance of a 30 GHz to 10 GHz regenerative frequency divider. The proposed divider design incorporates the conventional Miller regenerative frequency divider (divide-by-2) with an additional regenerative path. We achieve output referred
Nicholas G. Paulter Jr., Ioan Tudosa, Francesco Picariello, Pasquale Daponte, Luca De Vito, Sergio Rapuano
A prototype implementation of a phase measurement method (PMM) for a sine-wave signal delivered at the output port of a generator and its experimental assessment is presented. This PMM is capable of measuring the output phase of a sine-wave signal respect
Eliad Peretz, Peter Plavchan, Piotr Pachowicz, Jamie Tayar, Gerard van Belle, Greg Aldering, Angelle Tanner, Justin Albert, Daniel Huber, Leonard Hanssen, Brian Alberding, Joseph P. Rice, Steven West, John Mather, Allison Youngblood, Tabetha Boyajian, Brian Stalder, Jonathan Gagne, Susana Deustua, Kayla Carmical, Andrew Lewis
This paper describes the scientific and developmental aspects behind the QUAsi-Stationary Absolute Radiance (QUASAR) mission study. The scientific motivation on which the mission is built is established, including the absolute flux calibration of standard
Alexander Tzalenchuk, Nicolas Spethmann, Tim Prior, Jay H. Hendricks, Yijie Pan, Vladimir Bubanja, Guilherme Temporao, Dai-Hyuk Yu, Damir Ilic, Barbara L. Goldstein
Now that all base units are defined in terms of fundamental constants and can thus — at least in principle — be realized anytime and anywhere, rather than through a measurement chain leading back to unique physical artefacts, who holds the traceability
We present a simple method for the adjustment of an in-phase (I) and quadrature-phase (Q) Armstrong type modulator for use as a calibrator in precision noise metrology. The availability of relatively pure levels of both amplitude modulation (AM) and phase
Papa Amoah, Pentao Lin, Zeinab Mohammed Hassan, Rhonda Franklin, Engelbert Redel, Helmut Baumgart, Yaw S. Obeng
Changes in the chemo-electrical intrinsic properties of metal-oxide materials (MO) are commonly used as the basis of gas sensors. The most common gas sensors are based on chemically induced changes in electrical resistivity which necessarily involve making
For hydrogen-deuterium exchange mass spectrometry (HDX-MS) to have an increased role in quality control of biopharmaceuticals, H for D back-exchange occurring during protein analyses should be minimized to promote greater reproducibility. Standard HDX-MS