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Displaying 76 - 100 of 192

Marine Mammal Blubber Reference and Control Materials for Use in the Determination of Halogenated Organic Compounds and Fatty Acids

March 19, 2010
Author(s)
John R. Kucklick, Michele M. Schantz, Rebecca S. Pugh, Barbara J. Porter, Dianne L. Poster, Paul R. Becker, Teresa Rowles, Stefan D. Leigh, Stephen A. Wise
The National Institute of Standards and Technology (NIST) has a diverse collection of control materials derived from marine mammal blubber, fat, and serum. Standard Reference Material (SRM) 1945 Organics in Whale Blubber was recertified for polychlorinated

Uncertainties in Electron Probe Microanalysis

March 12, 2010
Author(s)
Ryna B. Marinenko, Stefan D. Leigh
This tutorial discusses the importance of citing valid uncertainties when reporting analytical results and the need for a universally accepted approach for evaluating uncertainties. Today, the CIPM procedure has been accepted by numerous international

Characterization of SiGe Films for use as a National Institute of Standards and Technology (NIST) Microanalysis Reference material (RM 8905)

February 1, 2010
Author(s)
Ryna B. Marinenko, Shirley Turner, David S. Simons, Savelas A. Rabb, Rolf L. Zeisler, Lee L. Yu, Dale E. Newbury, Rick L. Paul, Nicholas W. Ritchie, Stefan D. Leigh, Michael R. Winchester, Lee J. Richter, Douglas C. Meier, Keana C. Scott, D Klinedinst, John A. Small
Bulk SiGe wafers cut from single-crystal boules and two SiGe thick films (4 m and 5 m thick) on Si wafers were evaluated with the electron probe microanalyzer for the extent of heterogeneity and composition for use as reference materials needed by the

A Statistic That Identifies Errant Standard Preparation and Instrument Non-linearity Demonstrated With Mercury Standards Prepared by Blending NIST Fossil Fuel CRMs of Similar Matrices

November 16, 2009
Author(s)
Bruce S. MacDonald, John L. Molloy, Stefan D. Leigh, William R. Kelly, Andrew L. Rukhin
Interval-repeatability (Ir) is a statistic that users of certified reference materials (CRMs) may employ as a quality control check to identify incorrectly prepared working standards or nonlinear instrument response over a targeted concentration interval

Determination of Perfluorinated Alkyl Acid concentrations in Human Serum and Milk Standard Reference Materials

October 28, 2009
Author(s)
Jennifer M. Lynch, Antonia M. Calafat, Kayoko Kato, Mark E. Ellefson, William K. Reagen, Mark Strynar, Steven G. O'Connell, Craig M. Butt, Scott Mabury, Jeff Small, D.C.G. Muir, Stefan D. Leigh, Michele M. Schantz
Standard Reference Materials (SRMs) are homogeneous, well-characterized materials that are used to validate measurement methods and are critical in improving data quality. Disagreements in perfluorinated alkyl acid (PFAA) concentrations measured in

Effects of sample preparation on bacterial colonization of polymers

October 19, 2009
Author(s)
Diana N. Zeiger, Christopher Stafford, Yajun Cheng, Stefan D. Leigh, Sheng Lin-Gibson, Nancy Lin
Characterization of materials developed for medical usage frequently includes studies in which the materials are inoculated with bacteria in order to assess biofilm formation. Differences in the bacteria are considered to be due to the material alone; the

Report on Acceleration Comparison SIM.AUV.V-K1 - Draft B

March 20, 2009
Author(s)
David J. Evans, Adriana Hornikova, Stefan D. Leigh, Andrew L. Rukhin, William E. Strawderman
The first regional key comparison in vibration conducted under the auspices of the Inter-American System of Metrology (SIM) was begun in 1996. The comparison was registered with the International Bureau of Weights and Measures (BIPM) through the

Methodology for Evaluating Candidate Geometric Reference Scaffolds

November 1, 2007
Author(s)
Joy P. Dunkers, Stefan D. Leigh, David Dean, M Cooke, Richard Ketcham, Marcus T. Cicerone
The motivation for the work is to rank candidate reference scaffolds by quality metrics in a systematic and quantitative manner by screening several microstructural descriptors of importance. We chose total pore volume, pore volume distribution, and pore
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