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Reaction gas chromatography/mass spectrometry. 4—structure elucidation of cyclic sulphides by gas chromatography/mass spectrometry with the use of on-line hydrodesulphurization.

Published

Author(s)

Anzor I. Mikaia, Elena Trusova, Vladimir G. Zaikin, Naum Volinsky, Elena Karaulova, Gregory Galpern

Abstract

A GC-MS method is developed for structure determination of thiacyclanes. It is based on online gas- phase hydro- and deutero-desulfurization on Raney nickel after GC separation and before MS analysis.
Citation
Journal of Mass Spectrometry
Volume
19
Issue
9

Keywords

"GC-MS", "Online derivatization", "Hydrodesulfurization", "Cyclic sulfides"

Citation

Mikaia, A. , Trusova, E. , Zaikin, V. , Volinsky, N. , Karaulova, E. and Galpern, G. (1984), Reaction gas chromatography/mass spectrometry. 4—structure elucidation of cyclic sulphides by gas chromatography/mass spectrometry with the use of on-line hydrodesulphurization., Journal of Mass Spectrometry, [online], https://doi.org/10.1002/oms.1210190905 (Accessed May 26, 2024)

Issues

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Created September 1, 1984, Updated January 27, 2020