Mikaia, A.
, Smetanin, V.
, Zaikin, V.
and Vdovin, V.
(1985),
Reaction gas chromatography - mass spectrometry. Communication 5. Determination of the position of a double bond in alkenes using selective deuteration in the column of a gas Chromatograph-mass spectrometer., Russian Chemical Bulletin, [online], https://doi.org/10.1007/BF00947716
(Accessed October 10, 2025)
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Reaction gas chromatography - mass spectrometry. Communication 5. Determination of the position of a double bond in alkenes using selective deuteration in the column of a gas Chromatograph-mass spectrometer.
Published
Author(s)
, Vladimir Smetanin, Vladimir G. Zaikin, Valentin Vdovin
Abstract
A GC-MS method is developed for the determination of double bond location in alkenes based on comparative analysis of the mass spectra of corresponding alkanes and their vicinal Dideutero-analogs obtained via online hydrogenation and selective deuteration of alkenes in a specially developed reaction column.Citation
Russian Chemical Bulletin
Volume
34
Issue
3
Pub Type
Journals
Download Paper
Keywords
GC-MS, Electron ionization, Alkenes, Deuteration, Double bond location
Citation
Issues
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Created March 1, 1985, Updated January 27, 2020