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Reaction gas chromatography - mass spectrometry. Communication 5. Determination of the position of a double bond in alkenes using selective deuteration in the column of a gas Chromatograph-mass spectrometer.

Published

Author(s)

Anzor I. Mikaia, Vladimir Smetanin, Vladimir G. Zaikin, Valentin Vdovin

Abstract

A GC-MS method is developed for the determination of double bond location in alkenes based on comparative analysis of the mass spectra of corresponding alkanes and their vicinal Dideutero-analogs obtained via online hydrogenation and selective deuteration of alkenes in a specially developed reaction column.
Citation
Russian Chemical Bulletin
Volume
34
Issue
3

Keywords

GC-MS, Electron ionization, Alkenes, Deuteration, Double bond location

Citation

Mikaia, A. , Smetanin, V. , Zaikin, V. and Vdovin, V. (1985), Reaction gas chromatography - mass spectrometry. Communication 5. Determination of the position of a double bond in alkenes using selective deuteration in the column of a gas Chromatograph-mass spectrometer., Russian Chemical Bulletin, [online], https://doi.org/10.1007/BF00947716 (Accessed February 23, 2024)
Created March 1, 1985, Updated January 27, 2020