Nemsak, S.
, Strelcov, E.
, Guo, H.
, Hoskins, B.
, Duchon, T.
, Muller, D.
, Yulaev, A.
, Vlassiouk, I.
, Tselev, A.
and Kolmakov, A.
(2018),
In aqua electrochemistry probed by XPEEM: experimental setup, examples, and challenges, Topics in Catalysis, [online], https://doi.org/10.1007/s11244-018-1065-4, https://tsapps.nist.gov/publication/get_pdf.cfm?pub_id=924788
(Accessed October 7, 2024)
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In aqua electrochemistry probed by XPEEM: experimental setup, examples, and challenges
Published
Author(s)
Slavomir Nemsak, , , , Tomas Duchon, D Muller, , Ivan Vlassiouk, Alexander Tselev,
Abstract
Recent developments in environmental and liquid cells equipped with electron transparent graphene windows have enabled traditional surface science spectromicroscopy tools, such as XPS, PEEM, and SEM to be applied to study solid-liquid and liquid-gas interfaces. Here, we focus on the experimental implementation of PEEM to probe electrified graphene-liquid interfaces using electrolyte-filled microchannel arrays as a new sample platform. We demonstrate the important methodological advantage of these multi-sample arrays: they combine the wide field of view hyperspectral imaging capabilities from PEEM with the use of powerful data mining algorithms to reveal spectroscopic and temporal behaviors at the level of the individual microsample or the entire array ensemble.Citation
Topics in Catalysis
Volume
61
Issue
20
Pub Type
Journals
Download Paper
Keywords
XPEEM, multichannel arrays, in situ, electrochemistry, multivariate statistical analysis
Citation
Issues
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Created November 9, 2018, Updated October 12, 2021