East, K.
, Delaglio, F.
and Lisi, G.
(2021),
A Simple Approach for Reconstruction of Non-uniformly Sampled Psuedo-3D NMR Data for Accurate Measurement of Spin Relaxation Parameters, Journal of Biomolecular Nmr, [online], https://doi.org/10.1007/s10858-021-00369-7, https://tsapps.nist.gov/publication/get_pdf.cfm?pub_id=931975
(Accessed December 11, 2024)
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A Simple Approach for Reconstruction of Non-uniformly Sampled Psuedo-3D NMR Data for Accurate Measurement of Spin Relaxation Parameters
Published
Author(s)
Kyle East, , George Lisi
Abstract
We present a simple approach to reconstruction of NUS 2D spectral series as used in relaxation analysis. The approach treats this data as an ordinary 3D time-domain measurement whose imaginary part in the pseudo-dimension is zero, with familiar 3D NUS reconstruction methods such as IST applied accordingly. Best results on measured and simulated data were achieved using acquisitions with 9-to-12 planes and exponential spacing in the pseudo-dimension out to 2 times the inverse decay time. Given these criteria, the new approach can generate spectra reliably at sampling densities of 25% relative to a conventional measurement.Citation
Journal of Biomolecular Nmr
Volume
75
Pub Type
Journals
Download Paper
Keywords
Non-uniform sampling, spin relaxation, spectral reconstruction
Citation
Issues
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Created May 7, 2021, Updated November 29, 2022