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Search Publications by: Michael J. Fasolka (Fed)

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Displaying 1 - 25 of 134

Quantitative Subsurface Contact Resonance Force Microscopy of Model Polymer Nanocomposites

March 16, 2011
Author(s)
Jason P. Killgore, Jennifer Y. Kelly, Christopher M. Stafford, Michael J. Fasolka, Donna C. Hurley
We present experimental results on the use of quantitative contact resonance force microscopy (CR-FM) for mapping the planar location and depth of 50 nm silica nanoparticles buried beneath polystyrene films 30 nm to 165 nm thick. The presence of shallowly

Gradient Solvent Vapor Annealing of Block Copolymer Thin Films Using a Microfluidic Mixing Device

February 9, 2011
Author(s)
Kathryn L. Beers, Michael J. Fasolka, Julie N. Albert, Timothy D. Bogart, Ronald L. Lewis, J. Brian Hutchison, Bryan D. Vogt, Thomas H. Epps
Solvent vapor annealing (SVA) with solvent mixtures is a promising approach for controlling block copolymer thin film self-assembly. In this work, we present the design and fabrication of a solvent-resistant microfluidic mixing device to produce discrete

Investigation of Thermally Responsive Block Copolymer Thin Film Morphologies Using Surface Gradients

October 20, 2010
Author(s)
Jennifer Y. Kelly, Julie N. Albert, John A. Howarter, Shuhui Kang, Christopher Stafford, Thomas H. Epps, Michael J. Fasolka
We report the use of a gradient library approach to characterize the structure and behavior of thin films of a thermally-responsive block copolymer (BCP), poly(styrene-b-tert-butyl acrylate), that exhibits chemical deprotection and morphological changes

Measuring Up to Sustainable Water: Report from the 2010 NIST/Virginia Tech. Water Workshop

September 9, 2010
Author(s)
Lauren F. Greenlee, Jessica D. Torrey, Stephanie A. Hooker, Michael J. Fasolka, Sunil K. Sinha, Marc A. Edwards
Securing water sources of sufficient quality and quantity poses a major barrier to growing communities. Major investments in capitol and materials are planned in water treatment and distribution system infrastructure over the next several decades, but

Gradient and Microfluidic Library Approaches to Polymer Interfaces

January 1, 2010
Author(s)
Michael J. Fasolka, Christopher M. Stafford, Kathryn L. Beers
We present and overview of research conducted at the National Institute of Standards and Technology aimed at developing combinatorial and high throughput measurement approaches to polymer surfaces, interfaces and thin films. Topics include, 1) the

Quantifying Residual Stress in Nanoscale Thin Polymer Films via Surface Wrinkling

March 19, 2009
Author(s)
Jun Y. Chung, Thomas Q. Chastek, Michael J. Fasolka, Hyun W. Ro, Christopher Stafford
Residual stress, a pervasive consequence of solid materials processing, is stress that remains in a material after external forces have been removed. In polymeric materials, residual stress results from processes, such as film formation, that force and

Living Anionic Polymerization Using a Microfluidic Reactor

January 15, 2009
Author(s)
Thomas Q. Chastek, Kazunori Iida, Eric J. Amis, Michael J. Fasolka, Kathryn L. Beers, Jae H. Chun
Living anionic polymerizations were conducted within aluminum-polyimide microfluidic devices. Polymerizations of styrene in cyclohexane were carried out at various conditions, including elevated temperature (60 °C) and high monomer concentration (42 %, by