NOTICE: Due to a lapse in annual appropriations, most of this website is not being updated. Learn more.
Form submissions will still be accepted but will not receive responses at this time. Sections of this site for programs using non-appropriated funds (such as NVLAP) or those that are excepted from the shutdown (such as CHIPS and NVD) will continue to be updated.
An official website of the United States government
Here’s how you know
Official websites use .gov
A .gov website belongs to an official government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you’ve safely connected to the .gov website. Share sensitive information only on official, secure websites.
Combinatorial Edge Delamination Test for Thin Film Adhesion Concept, Procedure, Results
Published
Author(s)
Martin Y. Chiang, J He, R Song, Alamgir Karim, Wen-Li Wu, Eric J. Amis
Abstract
A high-throughput combinatorial approach to edge delamination test is proposed to map the failure of adhesion as a function of both temperature and film thickness in a single step. In this approach, a single specimen of a thin film bonded to a substrate with orthogonal thickness and temperature gradients is subdivided into separate samples. This approach can be adopted to measure the adhesion for films with thickness in the sub-micron range by the addition of an overlayer. Requirements for valid testing results from a mechanistic viewpoint are analyzed using three-dimensional computational fracture mechanics. An initial test result is presented to demonstrate the feasibility of the approach.
Proceedings Title
Fracture of Polymers, Composites and Adhesives, Conference | | | Elsevier
Chiang, M.
, He, J.
, Song, R.
, Karim, A.
, Wu, W.
and Amis, E.
(2003),
Combinatorial Edge Delamination Test for Thin Film Adhesion Concept, Procedure, Results, Fracture of Polymers, Composites and Adhesives, Conference | | | Elsevier, Diablerets, SZ, [online], https://tsapps.nist.gov/publication/get_pdf.cfm?pub_id=852169
(Accessed October 1, 2025)