NOTICE: Due to a lapse in annual appropriations, most of this website is not being updated. Learn more.

Form submissions will still be accepted but will not receive responses at this time. Sections of this site for programs using non-appropriated funds (such as NVLAP) or those that are excepted from the shutdown (such as CHIPS and NVD) will continue to be updated.

U.S. flag

An official website of the United States government

Official websites use .gov
A .gov website belongs to an official government organization in the United States.

Secure .gov websites use HTTPS
A lock ( ) or https:// means you’ve safely connected to the .gov website. Share sensitive information only on official, secure websites.

PUBLICATIONS

Soft X-ray Characterization Technique for Li Batteries under Operating Conditions

Published

Author(s)

Daniel A. Fischer, Cole Petersburg, Robert Daniel, Cherno Jaye, Faisal Alamgir

Abstract

O K edge and Co L edge near edge X-ray absorption fine structure (NEXAFS) was used to examine the cathode of an intact solid-state lithium ion battery. The novel technique allowed for the simultaneous acquisition of partial electron yield and fluorescence yield data during the first charge cycle of a LiCoO2-based battery below the intercalation voltage. The chemical environments of oxygen and cobalt at the surface are shown to differ chemically from those in the bulk. The present design enables a wide variety of in situ spectroscopies, microscopies, and scattering techniques.
Citation
Journal of Synchrotron Radiation
Volume
16
Pub Type
Journals

Download Paper

Local Download

Keywords

NEXAFS, XANES, Li ion battery, in situ, LiCoO2
Energy, Ceramics and Materials characterization

Citation

Fischer, D. , Petersburg, C. , Daniel, R. , Jaye, C. and Alamgir, F. (2009), Soft X-ray Characterization Technique for Li Batteries under Operating Conditions, Journal of Synchrotron Radiation, [online], https://tsapps.nist.gov/publication/get_pdf.cfm?pub_id=902383 (Accessed October 11, 2025)

Issues

If you have any questions about this publication or are having problems accessing it, please contact [email protected].

Created September 1, 2009, Updated February 19, 2017
Was this page helpful?