NOTICE: Due to a lapse in annual appropriations, most of this website is not being updated. Learn more.
Form submissions will still be accepted but will not receive responses at this time. Sections of this site for programs using non-appropriated funds (such as NVLAP) or those that are excepted from the shutdown (such as CHIPS and NVD) will continue to be updated.
An official website of the United States government
Here’s how you know
Official websites use .gov
A .gov website belongs to an official government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you’ve safely connected to the .gov website. Share sensitive information only on official, secure websites.
The effect of rough vs. smooth aggregate surfaces on the characteristics of the interfacial transition zone around a single spherical aggregate
Published
Author(s)
Edward Garboczi, Kai Lyu, Wei She, Changwen Miao
Abstract
Due to its higher porosity, the interfacial transition zone (ITZ) between cement paste and aggregates in cementitious composites is often viewed as a weak link in the microstructure. Sectional plane analysis based on back-scattered electron scanning electron microscope (BSE- SEM) images is used to quantify the ITZ porosity gradient, yet few researches have focused on the effect of aggregate surface morphology on the ITZ composition. In this paper, a model concrete specimen with a single spherical ceramic particle acting as an aggregate is used to study the properties of the ITZ and its uneven distribution around the aggregate based on quantitative analysis of BSE- SEM images. A careful treatment of the statistics of the ITZ were employed. The average porosity of the ITZ at a smooth part of the aggregate surface was smaller than that found at a rough part of the aggregate surface. A method is proposed to describe the local surface roughness (SR) at the pixel level, and relate this quantity to other ITZ properties. The relationship between the surface roughness and the ITZ porosity gradient within 30 m of the aggregate surface was analyzed with the "K-means" clustering method. The role of gravity was seen, since more porous ITZ regions tended to form underneath the aggregate than above the aggregate, with intermediate results at the aggregate sides.
Garboczi, E.
, Lyu, K.
, She, W.
and Miao, C.
(2019),
The effect of rough vs. smooth aggregate surfaces on the characteristics of the interfacial transition zone around a single spherical aggregate, Cement and Concrete Composites, [online], https://doi.org/10.1016/j.cemconcomp.2019.03.001, https://tsapps.nist.gov/publication/get_pdf.cfm?pub_id=926406
(Accessed October 2, 2025)