Joress, H.
, DeCost, B.
, Hassan, N.
, Braun, T.
, Gorham, J.
and Hattrick-Simpers, J.
(2022),
Development of an automated millifluidic platform and data-analysis pipeline for rapid electrochemical corrosion measurements: a pH study on Zn-Ni, Electrochimica Acta, [online], https://doi.org/10.1016/j.electacta.2022.140866, https://tsapps.nist.gov/publication/get_pdf.cfm?pub_id=934249
(Accessed October 21, 2025)
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Development of an automated millifluidic platform and data-analysis pipeline for rapid electrochemical corrosion measurements: a pH study on Zn-Ni
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Author(s)
, , Najlaa Hassan, , , Jason Hattrick-Simpers
Abstract
We describe the development of a millifluidic based scanning droplet cell platform for rapid and automated corrosion. This system allows for measurement of corrosion properties (e.g., open circuit potential, corrosion current through Tafel and linear polarization resistance measurements, and cyclic voltammograms) on a localized section of a planar sample. Our system is highly automated and flexible allowing for scripted changing and mixing of solutions and point-to-point motion on the sample. We have also created an automated data analysis pipeline. Here we demonstrate this tool by corroding a plate of electroplated \ceZn85Ni15} alloy at a range of pH and correlate our results with XPS measurements and literature.Citation
Electrochimica Acta
Pub Type
Journals
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Keywords
Scanning droplet cell, high-throughput, electrochemical corrosion, automation
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Created July 25, 2022, Updated November 29, 2022