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The Development of Microcalorimeter EDS Arrays

Published

Author(s)

Kent D. Irwin, James A. Beall, Steven Deiker, Gene C. Hilton, L. King, Sae Woo Nam, Dale Newbury, Carl D. Reintsema, John A. Small, Leila R. Vale

Abstract

High-energy-resolution cryogenic microcalorimeters are a powerful new tool for x-ray microanalysis. With demonstrated energy resolution 20 times better than with conventional semiconductor EDS, microcalorimeters are useful in applications such as nanoscale particle analysis. Unfortunately, single x-ray microcalorimeters are limited by low count rate (500 s-1) and small area (0.16 mm2). Both the count rate and the area can be improved by the implementation of arrays of microcalorimeters. In principle, this improvement in count rate and area comes without degraded energy resolution. The implementation of small microcalorimeter arrays will lead to improvements in the minimum detectable size of nanoscale particles and in the trace element concentration detection limit for a fixed analysis time. The development of kilopixel arrays capable of acquiring hundreds of thousands of counts per second, and with collecting areas of order 50 mm2, will make it possible to collect high-statistics spectra in small fractions of a second. This will make new applications possible, including real-time process-stream monitoring and the study of the evolution of film properties during deposition with x-ray fluorescence.
Citation
Microscopy and Microanalysis
Volume
8
Issue
suppl. 2

Keywords

EDS, microcalorimeter

Citation

Irwin, K. , Beall, J. , Deiker, S. , Hilton, G. , King, L. , Nam, S. , Newbury, D. , Reintsema, C. , Small, J. and Vale, L. (2002), The Development of Microcalorimeter EDS Arrays, Microscopy and Microanalysis (Accessed February 22, 2024)
Created October 31, 2002, Updated October 12, 2021