Crack Growth in Soda-Lime Silicate Glass Near the Static Fatigue Limit
Sheldon M. Wiederhorn, A Dretzke, J Rodel
The atomic force microscope (AFM) was used to explore the nature of features formed on the surfaces of cracks in soda-lime-silicate glass that were held at stress intensity factors below the crack growth threshold. All studies were conducted in water. Cracks were first propagated at a stress intensity factor above the crack growth threshold and then arrested for 16 h at a stress intensity factor below the threshold. The stress intensity factor was then raised to reinitiate crack growth. The cycle was repeated multiple times, varying the hold stress intensity factor, the hold time, and the propagation stress intensity factor. Examination of the fracture surface by optical microscopy showed surface features that marked the points of crack arrest during the hold time. These features were identical to those reported earlier by Michalske in a similar study of crack arrest. A study with the AFM showed these features to be a consequence of a bifurcation of the crack surface. During the hold period waviness developed along the crack front so that parts of the front propagated out of the original fracture plane, while other parts propagate into the plane. Crack growth changes from the original flat plane to a bifurcated surface with directions of as much as 3 to 5 to the original plane. This modification in the crack growth behavior cannot be explained by a variation in the far-field stresses applied to the crack. Nor can the crack growth features be explained by chemical fluctuations within the glass. We speculate that changes in crack growth direction are a consequence of an enhancement in the corrosion rate on the flank of the crack at stresses below the apparent crack growth threshold in a manner as described recently by Chuang and Fuller.
Journal of the American Ceramic Society
atomic force microscopy, crack growth, cracktips, glass, static fatigue