Certification of the Rheological Behavior of SRM 2490, Polyisobutylene Dissolved in 2,6,10,14-Tetramethylpentadecane

Published

February 1, 2002

Author(s)

Carl R. Schultesiz, C. Leighton

Abstract

The certification of the rheological properties of standard reference material SRM 2490, a non-Newtonian fluid consisting of polyisobutylene dissolved in 2,6,10,14-tetramethylpentadecane, is described. The viscosity and the first normal stress difference were measured in steady shear at rates between 0.001 s-1 and 100 s-1 at 0 C, 25 C and 50 C. The linear viscoelastic storage modulus G' and loss modulus G'' were also measured in dynamic oscillatory measurements between 0.04 rad/s and 100 rad/s in the temperature range between 0 C and 50 C and master curves calculated using time temperature superposition.

Citation

Special Publication (NIST SP) - 260-143

Report Number

260-143

Volume

34(24)

NIST Pub Series

Special Publication (NIST SP)

Pub Type

NIST Pubs

Download Paper

https://doi.org/10.6028/NIST.SP.260-143

Keywords

first normal stress difference, loss modulus, mastercurves, non-Newtonian, rheology, Standard Reference Material, storage modulus, time-temperature superposition, viscosity

Citation

Schultesiz, C. and Leighton, C. (2002), Certification of the Rheological Behavior of SRM 2490, Polyisobutylene Dissolved in 2,6,10,14-Tetramethylpentadecane, Special Publication (NIST SP), National Institute of Standards and Technology, Gaithersburg, MD, [online], https://doi.org/10.6028/NIST.SP.260-143 (Accessed December 4, 2024)