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Search Publications by: Katherine E. Sharpless (Fed)

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Displaying 76 - 100 of 129

Characterization of a Suite of Ginkgo-Containing Standard Reference Materials

September 1, 2007
Author(s)
Catherine A. Rimmer, S. Howerton, Katherine E. Sharpless, Lane C. Sander, Stephen E. Long, Karen E. Murphy, Barbara J. Porter, K. Putzbach, M. S. Rearick, Stephen A. Wise, Laura J. Wood, Rolf L. Zeisler, Diane K. Hancock, James H. Yen, J. M. Betz, A. NguyenPho, L. Yang, C. Scriver, S. N. Willie, R. Sturgeon, B. Schaneberg, C. Nelson, J. Skamarack, M. Pan, L. Kerri, D. Gray, E. H. Waysek, A. Blatter, E. Reich

Determination of Bitter Orange Alkaloids in Dietary Supplements Standard Reference Materials by Liquid Chromatography With Ultraviolet Absorbance and Fluorescence Detection

April 24, 2007
Author(s)
Karsten Putzbach, Katherine E. Sharpless, Lane C. Sander
Four adrenergic amines [(+/-) synephrine, (+/-) octopamine, tyramine, and n-methyltyramine) were determined in a variety of Citrus aurantium (Bitter Orange) containing dietary supplements. Two extraction techniques were evaluated in detail: Soxhlet

Determination of Caffeine, and Caffeine-Related Metabolites in Ephedra-Containing Standard Reference Materials Using Liquid Chromatography With Absorbance Detection and Tandem Mass Spectrometry

April 24, 2007
Author(s)
Jeanice M. Brown Thomas, Katherine E. Sharpless, S. Mitvalsky, Mark Roman, James H. Yen, Mary B. Satterfield
The concentration of caffeine and caffeine-related compounds in two ephedra-containing reference materials have been determined by three independent methods with measurements performed by the National Institute of Standards and Technology (NIST) and a

Preparation and Characterization of a Suite of Ephedra-Containing Standard Reference Materials

November 1, 2006
Author(s)
Katherine E. Sharpless, David L. Anderson, Therese A. Butler, J. M. Betz, Douglas A. Howell, S. G. Capar, J. Cheng, C. Fraser, G. Gardner, T. Ihara, J. W. Lam, Stephen E. Long, Elizabeth A. Mackey, M. McCooeye, Karen E. Murphy, W. R. Mindak, S. Mitvalsky, Karen W. Phinney, Barbara J. Porter, A. NguyenPho, Lane C. Sander, M. C. Roman, Mary B. Satterfield, Jeanice M. Brown Thomas, C. Scriver, R. E. Sturgeon, Robert D. Vocke Jr., Stephen A. Wise, Laura J. Wood, James H. Yen, L. Yang, G. C. Ziobro

Preparation and Characterization of a Suite of Ephedra-Containing Standard Reference Materials

June 1, 2006
Author(s)
Katherine E. Sharpless, D L. Anderson, J. M. Betz, Therese A. Butler, S. G. Capar, J. Cheng, C. Fraser, M. L. Gay, G. Gardner, D W. Howell, T. Ihara, J. W. Lam, Stephen E. Long, M. McCooeye, Elizabeth A. Mackey, W. R. Mindak, S. Mitvalsky, Karen E. Murphy, Karen W. Phinney, A. NguyenPho, Barbara J. Porter, M. C. Roman, Lane C. Sander, Mary B. Satterfield, C. Scriver, R. E. Sturgeon, Jeanice M. Brown Thomas, Robert D. Vocke Jr., Stephen A. Wise, Laura J. Wood, L. Yang, James H. Yen, G. C. Ziobro

k=2 and Other Sometimes Hidden Assumptions in Chemical Measurement Uncertainty Intervals

April 24, 2006
Author(s)
David L. Duewer, S L. Ellison, William F. Guthrie, D B. Hibbert, C Jackson, A Kallner, Stefan D. Leigh, Reenie M. Parris, Kenneth W. Pratt, Michele M. Schantz, Katherine E. Sharpless
A recent interlaboratory study that required individual analysts to estimate uncertainty intervals for their results revealed that some experienced chemical analysts have difficulty with measurement uncertainty calculations. To help validate assumptions

Dietary Supplement Standard Reference Materials

March 27, 2006
Author(s)
Lane C. Sander, Katherine E. Sharpless, Stephen A. Wise
A new category of Standard Reference Materials based on dietary supplements are under development by NIST, with certified values for organic constituents and selected trace elements. These materials are provided primarily for use in method development and