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1. Determination of Trace Sulfur in Biodiesel and Diesel Standard Reference Materials by Isotope Dilution Sector Field Inductively Coupled Plasma Mass Spectrometry
Topic: Inorganic Analytical Chemistry
Published: 11/14/2013
Authors: Steven J Christopher, Stephen E Long, Renata Amais, Joaquim N¿ga
Abstract: A method is described for quantification of sulfur at low concentrations on the order of 10 µg g-1 in biodiesel and diesel fuels using double isotope dilution and sector field inductively coupled plasma mass spectrometry (ID-SF-ICP-MS). Closed vessel ...
http://www.nist.gov/manuscript-publication-search.cfm?pub_id=912375

2. Isotope Dilution Mass Spectrometry For Quantitative Elemental Analysis Of Powdered Samples By Radiofrequency Pulsed Glow Discharge Time Of Flight Mass Spectrometry
Topic: Inorganic Analytical Chemistry
Published: 10/15/2013
Authors: John L Molloy, Julian Malherbe, Fanny Claverie, Beatriz Fernandez, Aitor Alvarez-Toral, Alfredo Sanz-Medel, Rosario Pereiro
Abstract: In recent years particular effort is being devoted to the development of pulsed glow discharges (PGDs) for mass spectrometry because this powering operation mode could offer important ionization analytical advantages. However, the capabilities of rad ...
http://www.nist.gov/manuscript-publication-search.cfm?pub_id=914387

3. Elemental analyses of soil and sediment fused with lithium borate using isotope dilution laser ablation-inductively coupled plasma-mass spectrometry (LA-ICP-IDMS)
Topic: Inorganic Analytical Chemistry
Published: 9/2/2013
Authors: John L Molloy, Julian Malherbe, Fanny Claverie, Aitor Alvarez-Toral, Beatriz Fernandez, Rosario Pereiro
Abstract: Quantitative analysis using Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICP-MS) remains challenging primarily due to elemental fractionation effects and to the lack of appropriate standards available for the wide variety of sample ...
http://www.nist.gov/manuscript-publication-search.cfm?pub_id=913550

4. Determination of Arsenic in Food and Dietary Supplement Standard Reference Materials by Neutron Activation Analysis
Topic: Inorganic Analytical Chemistry
Published: 9/1/2013
Author: Rick L Paul
Abstract: Arsenic has been measured in food and food supplement Standard Reference Materials by neutron activation analysis for the purpose of value-assigning As mass fractions and assessing homogeneity. Instrumental neutron activation analysis (INAA) has been ...
http://www.nist.gov/manuscript-publication-search.cfm?pub_id=910386

5. Fast standard addition method for LA-ICPMS using a spinning platform
Topic: Inorganic Analytical Chemistry
Published: 2/19/2013
Authors: John L Molloy, Stephen E Long, Fanny Claverie, Julian Malherbe, Naomi Bier
Abstract: A method has been developed for the fast and easy determination of Pb, Sr, Ba, Ni, Cu, and Zn, which are of geological and environmental interest, in solid samples by Laser Ablation Inductively Coupled Plasma Mass Spectrometry (LA-ICPMS) using a samp ...
http://www.nist.gov/manuscript-publication-search.cfm?pub_id=912435

6. Certification of NIST SRM 2569 Lead Paint Films for Children's Products
Topic: Inorganic Analytical Chemistry
Published: 10/15/2012
Authors: John L Molloy, John R Sieber, Karen E Murphy, Stephen E Long, Stefan D Leigh
Abstract: SRM 2569 Lead Paint Films for Children‰s Products is a new Standard Reference Material (SRM) developed for use primarily with XRF instrumentation. It consists of three paint coatings, with nominally 0 mg/kg, 90 mg/kg, and 300 mg/kg of Pb added, on p ...
http://www.nist.gov/manuscript-publication-search.cfm?pub_id=909911

7. Pilot Estuarine Mesocosm Study on the Environmental Fate of Silver Nanomaterials Leached from Consumer Products
Topic: Inorganic Analytical Chemistry
Published: 1/10/2012
Authors: Danielle Cleveland, Stephen E Long, Paul L. Pennington, Emily Cooper, Michael H. Fulton, Geoffrey I. Scott, Elijah J Petersen, Timothy M Brewer, Jeffrey M. Davis, Laura J Wood
Abstract: Although nanosilver consumer products (CPs) now enjoy widespread availability, little work has been done to determine the environmental fate and leaching of silver nanoparticles (AgNPs) from these products. This type of work is crucial, since the lif ...
http://www.nist.gov/manuscript-publication-search.cfm?pub_id=906343

8. Predictive Gold Nanocluster Formation Controlled by Metal-Ligand Complexes
Topic: Inorganic Analytical Chemistry
Published: 1/9/2012
Authors: John M Pettibone, Jeffrey W Hudgens
Abstract: The formation of ligand-protected transition metal nanoclusters in size-selective syntheses is driven by the inherent properties of the protecting ligands. We have previously reported the selective, monodisperse product formation of phosphine protect ...
http://www.nist.gov/manuscript-publication-search.cfm?pub_id=908225

9. Chromatographic Sample Collection from Two Phase (gas + liquid) Flows
Topic: Inorganic Analytical Chemistry
Published: 10/12/2011
Authors: Thomas J Bruno, Bret Windom
Abstract: A particularly challenging sample presentation in analytical chemistry is a flowing stream that consists of both a gas and liquid phase, in the situation in which an analysis is needed for both phases, separately. In these cases, the vapor and liqui ...
http://www.nist.gov/manuscript-publication-search.cfm?pub_id=908129

10. Characterization and Purification of Commercial SPS and MPS by Ion Chromatography and Mass Spectrometry
Topic: Inorganic Analytical Chemistry
Published: 1/21/2011
Authors: Ryan G. Brennan, Melissa Meaney Phillips, Liang Yueh Ou Yang, Thomas P Moffat
Abstract: SPS (bis-(3-sulfopropyl) disulfide) is an essential electrolyte additive used in the fabrication of copper interconnects by electrodeposition. The process is used over length scales ranging from on-chip Damascene wiring to through-silicon-vias for c ...
http://www.nist.gov/manuscript-publication-search.cfm?pub_id=906965



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