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NIST Polymer Mass Spectrometry Main Page

 MALDI Recipes Page Logo Synthetic Polymer MALDI Recipes Page

Standard Reference Database 172

Search for a synthetic polymer MALDI method from our list of recipes culled from the literature.


SRM 2881 Certificate  Absolute Molecular Mass Distribution Polymer Standard

Standard Reference Material 2881

For the accurate calibration of chromatography equipment and mass spectrometers.


Recommended Practice Guide Logo
Recommended Practice Guide

NIST Special Publication 960-21

Molecular Mass Distribution Measurement by Mass Spectrometry


Mass Spectrometry of Synthetic Polymers Workshops Logo
Mass Spectrometry of Synthetic Polymers Workshops

2008 Workshop Presentations
2005 Workshop Report
2004 Workshop Report
2003 Workshop Report
2002 Workshop Report


Selected Publications

Click on a title to view paper

"A General Method for the Quantitative Measurement of Molecular Mass Distribution by Mass Spectrometry", E.S. Park, W.E. Wallace, C.M. Guttman, K.M. Flynn, M.C. Richardson, G.A. Holmes, Journal of the American Society for Mass Spectrometry 20 (2009) 1638

"Quantitative Mass Spectrometry and Polydisperse Materials: Creation of an Absolute Molecular Mass Distribution Polymer Standard", C.M. Guttman, K.M. Flynn, W.E. Wallace, A.J. Kearsley, Macromolecules 42 (2009) 1695

"Quantitative Measurement of the Polydispersity in the Extent of Functionalization of Glass-Forming calix[4]resorcinarenes", W.E. Wallace, K.M. Flynn, C.M. Guttman, D.L. VanderHart, V.M. Prabhu, A. De Silva, N. Felix, C.K. Ober, Rapid Communications in Mass Spectrometry 23 (2009) 1957

"Matrix-Assisted Laser Desorption/Ionization Mass Spectrometry of Covalently Cationized Polyethylene as a Function of Sample Temperature", W.E. Wallace, W.R. Blair, International Journal of Mass Spectrometry 263 (2007) 82

"Numerical Optimization of Matrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry: Application to Synthetic Polymer Molecular Mass Distribution Measurement", W.E. Wallace, C.M. Guttman, K.M. Flynn, A.J. Kearsley, Analytica Chimica Acta 604 (2007) 62

"2,5 Dihydroxybenzoic Acid: Laser Desorption/Ionization as a Function of Temperature" W.E. Wallace, M.A. Arnould, R. Knochenmuss, International Journal of Mass Spectrometry 242 (2005) 13

"An Operator Independent Approach to Mass Spectral Peak Identification and Integration", W.E. Wallace, A.J. Kearsley, C.M. Guttman, Analytical Chemistry 76 (2004) 2446

"Optimizing the Covalent Cationization Method for the Mass Spectrometry of Polyolefins" S. Lin Gibson, L. Brunner, D.L. Vanderhart, B.J. Bauer, B.M. Fanconi, C.M. Guttman, W.E. Wallace, Macromolecules 35 (2002) 7149

"Molecular Structure of Silsesquioxanes Determined by Matrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry", W.E. Wallace, C.M. Guttman, J.M. Antonucci, Journal of the American Society for Mass Spectrometry 10 (1999) 224