Analytical Chemistry Division Publications in 2007

The following papers were published in 2008. If your institution subscribes to the journal named, clicking on an individual reference will direct you to the journal's website, where you can access the publication. If NIST has the right to post a reprint, clicking on the link will provide you with a pdf copy of the paper. [Note: Linking to these papers is currently in progress.]

Barker, L., Kelly, W. R., and Guthrie, W. F., “Determination of Sulfur in Biodiesel and Petroleum Diesel by X-Ray Fluorescence (XRF) Using the Gravimetric Standard Addition Method-II,” Energy Fuels, 22(4):2488-2490 (2007)

Bunk, D.M., “Reference Materials and Reference Measurement Procedures: An Overview from a National Metrology Institute,” Clin. Biochem. Rev., 28:131 (2007)

Camara, J. E., Satterfield, M. B., and Nelson, B. C., “Quantitative Determination of Disaccharide Content in Digested Unfragmented Heparin and Low Molecular Weight Heparin by Direct-Infusion Electrospray Mass Spectrometry,” J. Pharm. Biomed. Anal., 43(5):1706-1714 (2007)

Camara, J. E. and Hays, F. A., “Discrimination between Wild-Type and Ampicillin-Resistant Escherichia coli by Matrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry,” Anal. Bioanal. Chem., 389(5):1633-1638 (2007)

Cetiner, S. M., Unlu, K., and Downing, R.G., “Development of Time-of-Flight Neutron Depth Profiling at Penn State University,” J. Radioanal. Nucl. Chem. , 271(2):275-281 (2007)

Christopher, S. J., Pugh, R. S., Ellisor, M. B., Mackey, E. A., Spatz, R. O., Porter, B. J., Bealer, K. J., Kucklick, J. R., Rowles, T. K., and Becker, P. R., “Description and Results of the NIST/NOAA 2005 Interlaboratory Comparison Exercise for Trace Elements in Marine Mammals,” Accredit. Qual. Assur., 12(3-4):175-187 (2007)

Davis, W. C., Christopher, S. J., Pugh, R. S., Donard, O. F. X., Krupp, E. A., Point, D., Horvat, M., Gibicar, D., Kljakovic-Gaspic, Z., Porter, B. J., and Schantz, M. M., “Certification of Methylmercury Content in Two Fresh-Frozen Reference Materials: SRM 1947 Lake Michigan Fish Tissue and SRM 1974b Organics in Mussel tissue (Mytilus edulis),” Anal. Bioanal. Chem., 387(7):2335-2341 (2007)

Dodder, N. G., Tai, S., Sniegoski, L. T., and Welch, M. J., “Certification of Creatinine in a Human Serum Reference Material by GC-MS and LC-MS,” Clin. Chem., 53(9):1694-1699 (2007)

Dwyer, J. T., Holden, J., Andrews, K., Roseland, J., Zhao, C., Schweitzer, A., Perry, C. R., Harnly, J., Wolf, W., Picciano, M. F., Fisher, K., Saldanha, L. G., Yetley, E., Betz, J. M., Coates, P. M., Milner, J. A., Whitted, J., Burt, V., Radimer, K., Wilger, J., Sharpless, K. E., and Hardy, C. J., “Measuring Vitamins and Minerals in Dietary Supplements for Nutrition Studies in the USA,” Anal. Bioanal. Chem., 389(1):37-46 (2007)

Jackson, C. M., Esnouf, M. P., Winzor, D. J., and Duewer, D. L., “Defining and Measuring Biological Activity: Applying the Principles of Metrology,” Accred. Qual. Assur., 12(6):283-294 (2007)

Jones, B. J., Vergne, M. J., Bunk, D. M., Locascio, L. E., and Hayes, M. A., “Cleavage of Peptides and Proteins Using Light-Generated Radicals from Titanium Dioxide,” Anal. Chem., 79(4):1327-1332 (2007)

Kamande, M. W., Ross, D., Locascio, L. E., Lowry, M., and Warner, I.M., “Simultaneous Concentration and Separation of Coumarins Using a Molecular Micelle in Micellar Affinity Gradient Focusing,” Anal. Chem., 79(5):1791-1796 (2007)

Kucklick, J. R., Pugh, R. S., Becker, P. R., Schantz, M. M., Wise, S. A., and Rowles, T. K., “Description and Results of the 2005 NIST/NOAA Interlaboratory Comparison Exercise Program for Organic Contaminants in Marine Mammal Tissues,” NISTIR 7410, National Institute of Standards and Technology, Gaithersburg, MD (2007)

Liao, W. L., and Turko, I.V., “Separation of Stable Isotope-Labeled Unfolded Proteins before MALDI MS Analysis Enables Quantification of a Wide Range of Serum Proteins,” Mol. Cel. Proteomics, 6(8): B.12 , Suppl. S.. (2007)

Lindstrom, R. M., Zeisler, R., and Greenberg, R. R., “Accuracy and Uncertainty in Radioactivity Measurement for NAA,” J. Radioanal. Nucl. Chem., 271(2):311-315 (2007)

Lippa, K. A. and Schantz, M. M., “Microheterogeneity Evaluation of Polycyclic Aromatic Hydrocarbons in Particulate Standard Reference Materials,” Anal. Bioanal. Chem., 387(7):2389-2399 (2007)

Lippa, K. A., Rimmer, C. A., and Sander, L. C. “Shape Selectivity in Reversed-Phase Liquid Chromatography,” in: Advances in Chromatography, Grushka, E. and Grinberg, N., (Eds.); CRC Press, Taylor and Francis Group, Boca Raton, FL, Chapter 6, pp. 235-304 (2007)

Litz, J. L., Garrison, L., Fleber, L., Martinez, A., Contillo, J. P., and Kucklick, J. R., “Fine Scale Spatial Variation of Persistent Organic Pollutants in Bottlenose Dolphins (Tursiops truncatus) in Biscayne Bay, Florida,” Environ. Sci. Technol., 41(21):7222-7228 (2007)

Long, S. E., Davis, W. C., Day, R., Christopher, S. J., Mann, J. L., and Kelly, W. R., “Improved Certified Values for Total Mercury and Speciated Mercury in NIST Standard Reference Materials Using Isotope Dilution ICP-MS,” Am. Lab., 39(13):26-27(2007)

Mackey, E. A., Cronise, M. P., Fales, C. N., Greenberg, R. R., Leigh, S. D., Long, S. E., Marlow, A. F., Murphy, K. E., Oflaz, R., Sieber, J. R., Rearick, M. S., Wood, L. J., Yu. L. L., Wilson, S. A., Briggs, P. H., Brown, Z. A., Budahn, J., Kane, P. F., and Hall, W. L., Jr., “Development and Certification of the New SRM 695 Trace Elements in Multi-Nutrient Fertilizer,” Anal. Bioanal. Chem., 387(7):2401-2409 (2007)

Miller, W. R., and Guenther, F. R., “The Certification of a Nominal 20 mμ mol/mol H2S/N-2 Standard Reference Material Using Two Independent Methods,” Anal. Bioanal. Chem., 387(7):2433-2439 (2007)

Murphy, K. E., Long, S. E., and Vocke, R. D., “On the Certification of Cadmium at Trace and Ultratrace Levels in Standard Reference Materials Using ID ICP-MS,” Anal. Bioanal. Chem., 387(7): 2453-2461 (2007)

Nelson, B. C., Putzbach, K., Sharpless, K. E., and Sander, L. C., “Mass Spectrometric Determination of the Predominant Adrenergic Protoalkaloids in Bitter Orange (Citrus aurantium),” J. Agric. Food Chem., 55(24):9769-9775 (2007)

Peck, A. M., Kucklick, J. R., and Schantz, M. M., “Synthetic Musk Fragrances in Environmental Standard Reference Materials,” Anal. Bioanal. Chem., 387(7):2381-2388 (2007)

Phillips, K. M., Wolf, W. R., Patterson, K. Y., Sharpless, K. E., and Holden, J. M., “Reference Materials for Determination of the Nutrient Composition of Foods: Results from USDA's National Food and Nutrient Analysis Program,” Anal. Bioanal. Chem., 389(1):219-229 (2007)

Phillips, K. M., Wolf, W. R., Patterson, K. Y., Sharpless, K. E., Amanna, K. R., and Holden, J. M., “Summary of Reference Materials for the Determination of the Nutrient Composition of Foods,” Accredit. Qual. Assur., 12(3-4): 126-133 (2007)

Point, D., Davis, W. C., Ignacio Garcia Alonso, J., Christopher, S. J., Donard, O. F. X., and Wise, S. A., “Simultaneous Determination of Inorganic Mercury, Methylmercury and Total Mercury Concentrations in Cryogenic Fresh-Frozen and Freeze-Dried Biological Reference Materials,” Anal. Bioanal. Chem., 389(3):787-798 (2007)

Point, D., Davis, W. C., Christopher, S. J., Ellisor, M. B., Pugh, R. S., Donard, O. F. X., Becker, P. R., Porter, B. J., and Wise, S. A., “Development and Application of an Ultratrace Method for Speciation of Organotin Compounds in Cryogenically Archived and Homogenized Biological Materials,” Anal. Bioanal. Chem., 387(7):2343-2355 (2007)

Poster, D. L., Kucklick, J. R., Schantz, M. M., VanderPol, S. S., Leigh, S. D., and Wise, S. A., “Development of a House Dust Standard Reference Material for the Determination of Organic Contaminants,” Environ. Sci. Technol., 41(8):2861-2867 (2007)

Poster, D. L., Kucklick, J. R., Schantz, M. M., Porter, B. J., Sander, L. C., and Wise, S. A., “New Developments in Standard Reference Materials (SRMs) for Environmental Forensics,” Environ. Forensics, 8(1-2):181-191 (2007)

Pugh, R. S., Ellisor, M. B., Moors, A. J., Vander Pol, S. S., Day, R., Point, D., and Becker, P. R., “Current Avian Projects of the Marine Environmental Specimen Bank (Marine ESB), Charleston, SC, USA,” Cell Preserv. Technol., 5(1): 45-45 (2007)

Putzbach, K., Sharpless, K. E., and Sander, L. C., “Determination of Bitter Orange Alkaloids in Dietary Supplements Standard Reference Materials by Liquid Chromatography with Ultraviolet Absorbance and Fluorescence Detection,” J. Chromatogr. A., 1156(1-2):304-311 (2007)

Putzbach, K., Rimmer, C. A., Sharpless, K. E., Wise, S. A., and Sander, L. C., “Determination of Bitter Orange Alkaloids in Dietary Supplement Standard Reference Materials by Liquid Chromatography with Atmospheric-Pressure Ionization Mass Spectrometry,” Anal. Bioanal. Chem., 389(1):197-205 (2007)

Rimmer, C. A., Howerton, S. B., Sharpless, K. E., Sander, L. C., Long, S. E., Murphy, K. E., Porter, B. J., Putzbach, K., Rearick, M. S., Wise, S. A., Wood, L. J., Zeisler, R., Hancock, D. K., Yen, J. H., Betz, J. M., NguyenPho, A., Yang, L., Scriver, C., Willie, S., Sturgeon, R., Bland, B., Schaneberg, B., Nelson, C., Skamarack, J., Pan, M., Levanseler, K., Gray, D., and Waysek, E. H., “Characterization of a Suite of Ginkgo-Containing Standard Reference Materials,” Anal. Bioanal. Chem., 389(1):179-196 (2007)

Saupe, S. G. and Sharpless, K. E., “The Doctrine of Signatures Challenge,” Anal. Bioanal. Chem., 389(1):3-9 (2007)

Schantz, M. M., Keller, J. M., Kucklick, J. R., Poster, D. L., Stapleton, H. M., Vander Pol, S. S., and Wise, S. A., “New Standard Reference Material (SRM) 2585: Organic Contaminants in House Dust to Support Exposure Assessment Measurements,” Am. Lab., 39(15):22-28 (2007)

Schantz, M. M., Keller, J. M., Leigh, S. D., Patterson, Jr. D. G., Sharpless, K. E., Sjödin, A., Stapleton, H. M., Swarthout, R., Turner, W. E., and Wise, S. A., “Certification of SRM 1589a PCBs, Pesticides, PBDEs, and Dioxins/Furans in Human Serum,” Anal. Bioanal. Chem., 389(4):1201-1208 (2007)

Schantz, M. M., Brown Thomas, J. M., Poster, D. L., Sander, L. C., and Wise, S. A., “Spotlighting NIST Standard Reference Materials: New Solution Standard Reference Materials for Organic Constituents,” Am. Lab., 39(3):30-34 (2007)

Sharpless, K. E., Thomas, J. B., Duewer, D. L., Putzbach, K., Rimmer, C. A., Sander, L. C., Schantz, M. M., Wise, S. A., Yarita, T., and Yen, J. H., “Preparation and Characterization of Standard Reference Material 3276 Carrot Extract in Oil,” Anal. Bioanal. Chem., 389(1):207-217 (2007)

Sharpless, K. E., Thomas, J. B., Christopher, S. J., Greenberg, R. R., Sander, L. C., Schantz, M. M., Welch, M. J., and Wise, S. A., “ Standard Reference Materials for Foods and Dietary Supplements,” Anal. Bioanal. Chem., 389(1):171-178 (2007)

Sharpless, K. E. and Ulberth, F., “Food and Dietary Supplements,” Anal. Bioanal. Chem., 389(1):1-2 (2007)

Sieber, J.R., “Certified Reference Materials for Testing of Declarable Substances,” Am. Lab., 39(9):20-22 (2007)

Sieber, J. R., Mackey, E. A., Marlow, A. F., Paul, R. L., and Martin, R., “Validation of an Alkali Reaction, Borate Fusion, X-ray Fluorescence Method for Silicon Metal,” Powder Diffr., 22(2):146-151 (2007)

Simons, D. S., Downing, R. G., Lamaze, G. P., Lindstrom, R. M., Greenberg, R. R., Paul, R. L., Schiller, S. B., and Guthrie, W. F., “Development of Certified Reference Materials of Ion-Implanted Dopants in Silicon for Calibration of Secondary Ion Mass Spectrometers,” J. Vac. Sci. Technol., 25(4):1365-1375 (2007)

Stapleton, H. M., Keller, J. M., Schantz, M. M., Kucklick, J. R., Leigh, S. D., and Wise, S. A., “Determination of Polybrominated Diphenyl Ethers (PBDEs) in Environmental Standard Reference Materials,” Anal. Bioanal. Chem., 387(7):2365-2379 (2007)

Tai, S., Xu, B., Welch, M. J., and Phinney, K. W., “Development and Evaluation of a Candidate Reference Measurement Procedure for the Determination of Testosterone in Human Serum Using Isotope-Dilution Liquid Chromatography-Tandem Mass Spectrometry,” Anal. Bioanal. Chem., 388(5-6):1087-1094 (2007)

Tewari, Y. B., Liebman, J. F., Rozzell, J. D., Vanderah, D. J., Schantz, M. M., “A Thermodynamic Study of Ketoreductase-Catalyzed Reactions 4. Reduction of 2-Substituted Cyclohexanones in N-Hexane,” J. Chem. Thermodynamics, 39(7):1090-1097 (2007)

Thomas, J. B., Sharpless, K. E., Mitvalsky, S., Roman, M., Yen, J., and Satterfield, M. B., “Determination of Caffeine and Caffeine-Related Metabolites in Ephedra-Containing Standard Reference Materials Using Liquid Chromatography with Absorbance Detection and Tandem Mass Spectrometry,” J. AOAC Int., 90(4): 934-940 (2007)

Tremsin, A. S., Hussey, D. S., Downing, R. G., Feller, W. B., Mildner, D. F. R., Jacobson, D. L., Arif, M., and Siegmund, O. H. W., “Neutron Collimation with Microchannel Plates: Calibration of Existing Technology and Near Future Possibilities,” IEEE Trans. Nucl. Sci., 54(2):362-366 (2007)

Vander Pol, S. S., Ellisor, M. B., Pugh, R. S., Becker, P. R., Poster, D. L., Schantz, M. M., Leigh, S. D., Wakeford, B. J., Roseneau, D. G, and Simac, K. S., “Development of a Murre (Uria spp.) Egg Control Material,”Anal. Bioanal. Chem., 387(7):2357-2363 (2007)

Vitzthum, F., Siest, G., Bunk, D. M., Preckel, T., Wenz, C., Hoerth, P., Schulz-Knappe, P., Tammen, H., Adamkiewicz, J., Merlini, G., and Anderson, N.L., “Metrological Sharp Shooting for Plasma Proteins and Peptides: The Need for Reference Materials for Accurate Measurements in Clinical Proteomics and In Vitro Diagnostics to Generate Reliable Results,” Proteomics Clin. Appl., 1(9):1016-1035 (2007)

White V. E., Phinney, K. W., Porter, B. J., Sander, L. C., Christensen, R. G., Waddell, J., Fatah, A. A., and Thompson, R. Q., “Oleoresin Capsicum Canister Study,” NISTIR 7486, National Institute of Standards and Technology, Gaithersburg, MD (2007)

Wise, S. A. and Emons, H., “10th International Symposium on Biological and Environmental Reference Materials (BERM 10),” Anal. Bioanal. Chem., 387(7):2309-2311 (2007)

Yu, L. L., Wood, L. J., Kelly, W. R., and Turk, G. C., “Determination of Be in Alumina by ICP-OES After Carius Tube Digestion,” J. Anal. At. Spectrom., 22(11):1427-1429 (2007)

Zhao, L., Robinson, L., Paul, R.L., Greenberg, R.R., and Miao, S.L., “Application of Cold Neutron Prompt-Gamma Activation Analysis in Environmental Studies of Aquatic Plants,” J. Radioanal. Nucl. Chem., 271(3):777-782 (2007)

Zhao, L., Robinson, L., Paul, R.L., Greenberg, R.R., and Miao, S.L., Erratum to “Determination of Carbon, Nitrogen and Phosphorus in Cattail Using Cold Neutron Prompt-Gamma Activation Analysis,” J. Radioanal. Nucl. Chem., 273(2):513(2007)

Zhao, W., Golding, T. D., Littler, C. L., Dinan, J. H., Dura, J. A., and Lindstrom, R. M., “Diffusion of Selenium in Liquid-Phase Epitaxy–Grown Hg0.78Cd0.22Te,” J. Electron. Matls.36(8):822-825(2007)