NIST Administrative Manual, Subchapter 4.09
Transmittal Date - 12/21/93
APPENDIX E
STATEMENTS OF UNCERTAINTY ASSOCIATED WITH MEASUREMENT RESULTS
A measurement result is complete only when accompanied by a quantitative
statement of its uncertainty. This policy requires that NIST measurement
results be accompanied by such statements and that a uniform approach to
expressing measurement uncertainty be followed.
1. Background
Since the early 1980's, an international consensus has been developing
on a uniform approach to the expression of uncertainty in measurement.
Many of NIST's sister national standards laboratories as well as a number
of important metrological organizations, including the Western European
Calibration Cooperation (WECC) and EUROMET, have adopted the approach recommended
by the International Committee for Weights and Measures (CIPM) in 1981
[1] and reaffirmed by the CIPM in 1986 [2].
Equally important, the CIPM approach has come into use in a significant
number of areas at NIST and is also becoming accepted in U.S. industry.
For example, the National Conference of Standards Laboratories (NCSL) is
using it to develop a Recommended Practice on measurement uncertainty for
NCSL member laboratories.
The CIPM approach is based on Recommendation INC-1 (1980) of the Working
Group on the Statement of Uncertainties [3]. This group was convened in
1980 by the International Bureau of Weights and Measures (BIPM) in response
to a request by the CIPM. More recently, at the request of the CIPM, a
joint BIPM/IEC/ISO/OIML working group developed a comprehensive reference
document on the general application of the CIPM approach titled Guide
to the Expression of Uncertainty in Measurement [4] (IEC: International
Electrotechnical Commission; ISO: International Organization for Standardization;
OIML: International Organization of Legal Metrology). The development of
the Guide is providing further impetus to the worldwide adoption
of the CIPM approach.
2. Policy
All NIST measurement results are to be accompanied by quantitative statements
of uncertainty. To ensure that such statements are consistent with each
other and with present international practice, this NIST policy adopts
in substance the approach to expressing measurement uncertainty recommended
by the International Committee for Weights and Measures (CIPM). The CIPM
approach as adapted for use by NIST is:
1) Standard Uncertainty: Represent each component of uncertainty
that contributes to the uncertainty of the measurement result by an estimated
standard deviation ui, termed standard uncertainty, equal
to the positive square root of the estimated variance u.
2) Combined Standard Uncertainty: Determine the combined standard
uncertainty uc of the measurement result, taken to represent
the estimated standard deviation of the result, by combining the individual
standard uncertainties ui (and covariances as appropriate) using
the usual ``root-sum-of-squares'' method, or equivalent established and
documented methods.
Commonly, uc is used for reporting results of determinations
of fundamental constants, fundamental metrological research, and international
comparisons of realizations of SI units.
3) Expanded Uncertainty: Determine an expanded uncertaintyU
by multiplying uc by a coverage factor k: U
= k uc . The purpose of U is to provide an interval yU
to y + U about the result y within which the value
of Y, the specific quantity subject to measurement and estimated
by y, can be asserted to lie with a high level of confidence. Thus
one can confidently assert that y U Y y + U,
which is commonly written as
Y = y U.
Use expanded uncertainty U to report the results of all NIST
measurements other than those for which uc has traditionally been
employed. To be consistent with current international practice, the value
of k to be used at NIST for calculating U is, by convention,
k
= 2. Values of k other than 2 are only to be used for specific applications
dictated by established and documented requirements.
4) Reporting Uncertainty: Report U together with the coverage
factor k used to obtain it, or report uc .
When reporting a measurement result and its uncertainty, include the
following information in the report itself or by referring to a published
document:
- A list of all components of standard uncertainty, together with their
degrees of freedom where appropriate, and the resulting value of uc.
The components should be identified according to the method used to estimate
their numerical values:
A. those which are evaluated by statistical methods,
B. those which are evaluated by other means.
- A detailed description of how each component of standard uncertainty
was evaluated.
- A description of how k was chosen when k is not taken
equal to 2.
It is often desirable to provide a probability interpretation, such
as a level of confidence, for the interval defined by U or
uc.
When this is done, the basis for such a statement must be given.
Additional guidance on the use of the CIPM approach at NIST may be found
in Guidelines for Evaluating and Expressing the Uncertainty of NIST
Measurement Results [5]. A more detailed discussion of the CIPM approach
is given in the Guide to the Expression of Uncertainty in Measurement
[4]. Classic expositions of the statistical evaluation of measurement processes
are given in references [6-8].
3. Responsibilities
a. Operating Unit Directors are responsible for compliance with this
policy.
b. The Statistical Engineering Division, Computing and Applied Mathematics
Laboratory, is responsible for providing technical advice on statistical
methods for evaluating and expressing the uncertainty of NIST measurement
results.
c. NIST Editorial Review Boards are responsible for ensuring that statements
of measurement uncertainty are included in NIST publications and other
technical outputs under their jurisdiction which report measurement results
and that such statements are in conformity with this policy.
d. The Calibration Advisory Group is responsible for ensuring that calibration
and test reports and other technical outputs under its jurisdiction are
in compliance with this policy.
e. The Standard Reference Materials and Standard Reference Data programs
are responsible for ensuring that technical outputs under their jurisdiction
are in compliance with this policy.
f. Authors, as part of the process of preparing manuscripts and other
technical outputs, are responsible for formulating measurement uncertainty
statements consistent with this policy. These statements must be present
in drafts submitted for NIST review and approval.
4. Exceptions
It is understood that any valid statistical method that is technically
justified under the existing circumstances may be used to determine the
equivalent of ui , uc , or U. Further, it is recognized
that international, national, or contractual agreements to which NIST is
a party may occasionally require deviation from this policy. In both cases,
the report of uncertainty must document what was done and why.
5. References Cited
[1] CIPM, BIPM Proc.-Verb. Com. Int. Poids et Mesures 49,
8-9, 26 (1981) (in French); P. Giacomo, ``News from the BIPM,'' Metrologia18,
41-44 (1982).
[2] CIPM, BIPM Proc.-Verb. Com. Int. Poids et Mesures 54,
14, 35 (1986) (in French); P. Giacomo, ``News from the BIPM,'' Metrologia24,
45-51 (1987).
[3] R. Kaarls, ``Rapport du Groupe de Travail sur l'Expression des Incertitudes
au Comité International des Poids et Mesures,'' Proc.-Verb. Com.
Int. Poids et Mesures 49, A1-A12 (1981) (in French); P. Giacomo,
``News from the BIPM,'' Metrologia 17, 69-74 (1981). (Note
that the final English-language version of Recommendation INC-1 (1980),
published in an internal BIPM report, differs slightly from that given
in the latter reference but is consistent with the authoritative French-language
version given in the former reference.)
[4] ISO, Guide to the Expression of Uncertainty in Measurement,
prepared by ISO Technical Advisory Group 4 (TAG 4), Working Group 3 (WG
3), October 1993. ISO/TAG 4 has as its sponsors the BIPM, IEC, IFCC (International
Federation of Clinical Chemistry), ISO, IUPAC (International Union of Pure
and Applied Chemistry), IUPAP (International Union of Pure and Applied
Physics), and OIML. Although the individual members of WG 3 were nominated
by the BIPM, IEC, ISO, or OIML, the Guide is published by ISO in
the name of all seven organizations. NIST staff members may obtain a single
copy of the Guide from the Calibration Program.
[5] B. N. Taylor and C. E. Kuyatt, Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results, NIST Technical
Note 1297, prepared under the auspices of the NIST Ad Hoc Committee on
Uncertainty Statements (U.S. Government Printing Office, Washington, DC,
January 1993).
[6] C. Eisenhart, ``Realistic Evaluation of the Precision and Accuracy
of Instrument Calibration Systems,'' J. Res. Natl. Bur. Stand. (U.S.)
67C,
161-187 (1963). Reprinted, with corrections, in Precision Measurement
and Calibration: Statistical Concepts and Procedures, NBS Special Publication
300, Vol. I, H. H. Ku, Editor (U.S. Government Printing Office, Washington,
DC, 1969), pp. 21-48.
[7] J. Mandel, The Statistical Analysis of Experimental Data
(Interscience-Wiley Publishers, New York, NY, 1964, out of print; corrected
and reprinted, Dover Publishers, New York, NY, 1984).
[8] M. G. Natrella, Experimental Statistics, NBS Handbook 91 (U.S. Government Printing Office, Washington, DC, 1963; reprinted October 1966 with corrections).